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TỔNG HỢP, NGHIÊN CỨU CẤU TRÚC PHỨC CHẤT CỦA NIKEN(II) VÀ PALADI(II) VỚI 4-PHENYL THIOSEMICACBAZON AXETOPHENON

Trịnh Ngọc Châu, Nguyễn Thị Bích Phương, Nguyễn Văn Hà

Abstract


This paper reports the synthesis and spectral studies of palladium and nickel with acetophenone 4-phenyl thiosemicarbazones (Hpthacp). The ligand and complexes are characterized by means of chemical analysis, IR, ESI-MS and 1H-NMR spectroscopy. The obtained data show that in M(pthacp)2 (M: Ni, Pd) complexes, the ligand acts as anionic bidentate ligands, two coordinate bonds realize through S and N(1) atoms.

Keywords: Palladium complex; 4-phenyl thiosemicarbazone.


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